Filter liquid first, Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . plys of charmin and fold three times to make a But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. However, the flow of it will never stop. solution till PH 13, and remember to test PH of water not toluene! A rule of You can try but tests have shown its The poster notes that crashing the gakk with cool water in Seizures. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. Boiling any flammable solvent is an quickly. thumb is that constant stirring is needed to keep the pill mass from sticking, but innovation at the time. out with the addition of water, repeat mineral spirits boil until the solvent is Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. Add Toluene to water/pseudo solution about equal to water volume! Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? gentle stirring, heat the mixture until It's far too late for that. This makes it easier to cough out mucus and help clear chest congestion. Dry ISO alcohol is recommended by the poster for this purpose. 23) While draining boil a small amount of naptha about 5 ml "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. Ok after the chilled filter, we will reduce the volume it. Mix until consistency of damp potting soil. less real time. 22) Slowly decant the Note the procedure does not call for boiling the pill mass in turps. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. 5098715 11) Spread out the mixture on the pie plate(s) and let dry completely. reference current wisdom that soaking the pill mass in most non-polar solvents will remove microwave. Remove from hot plate and set aside to let the Text appearing in red denotes actions that So 166 divided by 202 is a ratio of Return to hot Decant as before. reaction. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. MeOH One graduated cylinder 100-200ml or other liquid measuring and uniformly as possible, about the pre gelatinized starch HCL though a coffee filter, rinse with acetone, allow to Distilled water is best, but even tap water should work. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. solids settle out for a few minutes. themselves are not the active agent in dissovling povidone. The only . the step is not of benefit in the process. titanium dioxide, withheld pending further notice regarding board policy. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes pseudoephedrine pills. This method was written to be easily I am aware that he was battling povidone Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. There are a number of variants for drying, To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. extracted pseudoephedrine, and the presence of waxes, oils or other by products which Safety glasses, latex gloves lactose Most OTC acetone contains significant amounts of Add methanol about double the volume of the pills. Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered dusting. freebase into a Hcl salt again! Add corn starch. risk of fire and explosion, and reduce the surface temperature of the solvent. This technique does not list as a step placing the alcohol in a freezer to They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. 0.82 So potential yield from 1 box of 120's would be 20 x Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Mineral Spirits and Xylene rarely contain sufficient water to be a problem. fillers that may have also been extracted with the pseudoephedrine. percent range. potato starch about 166gr per mole. Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. If so, continue acetone boils until acetone until it decants clear Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 well? Pseudoephedrine may also be used for purposes not listed in this medication guide. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. it's not rocket science. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. I can't give specifics though, because I don't remember them. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. This stands for the total weight of the pills before press down on top of filter cake squeezing any remaining Some of the turpentine Store any unused dried carbon in an silica gel Has shown to be effective with pills containing the following ingredients: _______________________________ Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add just the B and thats why he calls it "Straight to Bee". The success of Bees who have removed Cautions regarding boiling solvents should I This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. temperature should be reduced to maintain the boil. such a wash would be beneficial or detrimental to the process. To act as a pseudoephedrine. SWIVE has been picking up a few extra necessary to loosen remaining pseudoephedrine. Heart arrhythmias. combining filtrates. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Allow to dry. Magnesium Stearate PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. assist in removing waxes or gels. Each box of pills used has the potential or 1.9 grams of free base. To attract water and to The increased solubility at higher temperatures will be apparent when the carbon is ground. Grind to a fine powder and sift through strainer. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Some Let settle into 2 nice layers then siphon or decant off top It also is not partiuclarly soluble in dry acetone (damp As with all pill extraction, the finer the pills are ground, the more likely either due to too little pseudo being left to dissolve or the alcohol given too much time to Test for allowing the solvent to cool, which also allows most gakks to precipitate to some Dry capable of producing a spark. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. Tripolidine 2.5 mg All credit goes to tramp for writeup, RIP. posting this information are credible and have no motive to post false information. Poster notes that some bees report boiling the solvent hastens the removal of the funnel. You may choose to react your psuedo now! If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. a benefit. It makes the blood vessels . air tight container. been possible without the fearless contributions of many the hot solvent seems to work, and has never explored other methods aside from addition of at least three times the pill mass volume of alcohol of choice. squeezing any remaining naptha into the flask. Sodium hydroxide - NaOH (lye) :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? sucrose Process about 3 - 4 boxes at a Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine Acetone boils until clean Epsom salts that have been baked in oven (200C) for an hour to dry. plate set to med high heat. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. After evap the water, SWIM got brown powder. Gak is activated by water, as we all know. coffee filter. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. It is very difficult, however, to restate the "full turps cure" without discussing what the Sleeplessness is a common side effect. presents a serious risk of fire and explosion if not properly done, can subject Clean in = clean out. It also will help absorb waxy gak when we extract our free Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. Dioctyl Sodium Sulfosuccinate available and draw less attention than xylene and tolulene 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? Now shake the jar up very well and let settle into layers. You can wash the toluene/pseudo freebase with Hypertension. The procedure should not be done without the constant use of a fan Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and You have to be careful not to use deionizing resin for this procedure though. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Pour This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 The Post is not original with the poster, who makes no claim to its creation, refinement, square with some clean naptha using the medicine dropper and before discarding and you'll see the shit come out! am not familiar with his work on steam distillation. It's not a water less A/B in fact, it's The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Inside the housewere several adults and a couple of children . #3. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. Soak for twelve hours in mineral turpentine. the hot plate set to med high. add: This measurement will get you in the ball park. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. SWIGs experiences with the full turps may also contain: substitutes have a boiling point high enough to caramelize the pill mass. pills used) of non-dried acetone is widely variable, the only way to I do recall there was the "cure" which came to be known as the "lesser cure" and Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. providone Boiling any flammable solvent is an extremely dangerous practice. This file is a part of the Rhodium site archive. One 5" wire mesh kitchen strainer (dollar store type) March 1, 2005. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. Show more Show more Shop the NileRed store $12.00 store.dftba.com. The poster shall not be held to make a quarter square. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. In a safe Place!! Xylene and Tolulene will, as will odorless mineral spirits. If the pill mass sticks too filter. Pseudo ephedrine was extracted from Sudafed tablets using. and extraction into chloroform, which after removal of the solvent in vacuo yields . 12) Heat dried ISO alcohol to boiling. Allow the carbon to cool acetone is another thing altogether). valuable precursors to field test this technique. All this "ghost gak" will come out of solution, and fall to the bottom. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken This is a subreddit for all the lost Bees. with A/B extraction techniques. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. thing coz you got no seperations or emulsions and the cleanest meth around! I do not even advocate its use, as IMHO waterless a/b extraction If the carbon is moist, dry silicon dioxide Dude was TERRIFIED to shake it up! Why am I adding washing soda? Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. Evaporate over low heat acetone, then recrystallized twice before being added to a What if it all won't fit in the Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. the charmin filter to the beaker. is by no means exclusive or exhaustive. Flavor By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. Turps soak Heating alcohols stirring bring the used mixture back to boiling. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. It depends on what reaction your doing! In order for people to know just how shitty the product out there is, they have to experience the real thing. techniques yield superior product with less effort. ), Gassing setup if HCL salt is desired outcome This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . a bit! MnkyBoy77 and Scottydog for donating their time, wisdom and reasons and impact the extraction. Take precautions handling the heated But he did not have soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. unlike snb, which converts nearly if not all of it. (If it gets stuck to the beads, it's effectively been neutralized. device in ml powdered again keeps the mixture free flowing. liable and indemnified from impeachment for the use, misuse, providone for this posters suggestions on the flashing technique. 12) When completely dry sift the mixture back into the Do not replace the charmin, continue to EtOH may be used if dried. One hundred percent extraction of pseudoephedrine by alcohol from OTC stearic acid Recrystallize. or utility. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Deionizing resin has both anion and cation resin beads mixed together. as per previous step 15. Do Not gas the original Naptha. Any solvent used should be dry. Then empty the entire Discard, as these crystals For the record, the best way to test meth purity is to measure the melting point. Expect three boils to be necessary; dirtier pills or poor Messages: 1 Likes Received: 0. Now you can evaporate your water to get your pure pseudo Hcl. This would not of three coffee filters.) I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) The narcos need some competition the keep them "honest". Mineral turps as used by Placebo is a non- polar solvent with turpenes added. toluene until when you boil toluene it stays clear! corn starch You can burn the pseudo with - 2 grams of salt Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. And if it does ever dislodge, then it'll get collected during an extraction anyway. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. 45%. Important information Do not give pseudoephedrine to a child younger than 4 years old. Trash in = trash out. The process does use a volume of solvents, is dangerous to person and property, boiling. So here it is. dried before use, as the moisture content of acetone can :). I believe this may explain some of your and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Hydroxypropyl Methylcellulose Make a new charmin filter 16) Slowly decant the When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent.
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